Document Details

Document Type : Article In Journal 
Document Title :
Electrodeposition and morphology analysis of nickel nanoparticles from sulphate bath
Electrodeposition and morphology analysis of nickel nanoparticles from sulphate bath
 
Subject : Chemistry 
Document Language : English 
Abstract : The electrodeposition of Nickel in the presence of organic compound was studied systematically as function of the nature of the organic additive. The effects of various parameters such as nickel sulphate concentration, bath temperature, current density have been investigated on deposit physical appearance. The tolerance limits and the effect of combined organic additive have been identified under different experimental conditions. We have used scanning electron microscopy (SEM) to characterize the surface morphology of deposits. The SEM pictures show the formation of domain growth of nickel in which nanoparticles are mostly concentrated at domain boundaries and incorporated in the coating matrix to improve the surface mechanical properties. The coatings are found to be highly adherent and uniform by adding calixarene derivative as organic additive at very low concentration. Threedimensional AFM images confirm that the presence of calixarene derivative improves the surface smoothness. The microhardness measurements were performed and the structure of deposits was examined by X-ray diffraction. 
ISSN : 1348-0391 
Journal Name : e-Journal of Surface Science and Nanotechnology 
Volume : 8 
Issue Number : 2010 
Publishing Year : 1431 AH
2010 AD
 
Article Type : Article 
Added Date : Wednesday, November 16, 2011 

Researchers

Researcher Name (Arabic)Researcher Name (English)Researcher TypeDr GradeEmail
Kamel BelhamelBelhamel, Kamel ResearcherDoctoratekbelhamel@yahoo.fr
Hamid KherazKheraz, Hamid ResearcherDoctorate 
Rainer LudwigLudwig, Rainer ResearcherDoctorate 
T. K Dzung NguenNguen, T. K DzungResearcherDoctorate 
Nicholas AllsopAllsop, Nicholas ResearcherDoctorate 
صالح سالم الجعيدAl-Juaid, Salih SResearcherDoctoratesaljuaid@kau.edu.sa

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